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Analyse This provides a useful resource for all scientists working in chemical analysis. It is sent out to subscribers on a regular basis. All past editions of Analyse This can be accessed on this page.

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2014

April

Upcoming MTS Courses; Revision of EU GMP Chapter 6: Quality Control - Effective from 1st October 2014; The Nature of 'Error' in Analytical Testing; MTS Helpdesk: Do I need to revalidate my method if I change the column?; MTS Recommends... Current Practices and Considerations for a Stability-Indicating Method in Pharmaceutical Analysis

March

Upcoming MTS Courses; New Method Validation Guidance from FDA; Free Tools Update!; MTS Helpdesk: For How Long Should I Equilibrate My HPLC Column?; MTS Recommends... Complying with Revised USP Chapters on Weighing

January

Replicates in Analytical Methods - When and How Many?; Training Courses on Method Validation and Transfer in Dublin - March 2014; MTS Helpdesk: How long should it take to purge the lines on my HPLC system?; MTS Recommends... More Myths in Ultrahigh-Pressure Liquid Chromatography


2013


November

6 Reasons to join MTS in Berlin this December; Limit of Quantification: Does it Matter? MTS Course Calendar 2014; MTS Helpdesk: Help on... When should I throw my HPLC column away? Auditing and consultancy services from MTS; MTS Recommends... Why do I have carryover?

October


Develop Your Expertise in Analytical Methods - Training Courses Coming Up; Free Download: Aide Memoire for Analytical Method Transfer Is Your Analytical Method Stability Indicating?; Auditing and Consultancy Services from MTS: MTS Helpdesk: Help on... Do I need Linearity, Accuracy and Precision for an Area % Method?; MTS Recommends... The Top 10 HPLC and UHPLC Column Myths

March

MTS Helpdesk: Help on... Validation Shoes that Method is not Linear Through Zero; Early Booking Deadlines Coming Up; HPLC Troubleshooting Tip: Preventing Mobile Phase Problems when using TFA; Update to Chapter 6 of the EU GMP Guidelines - Part 2; HPLC Training in Dublin - May 2013; MTS Recommends... Getting it Write

February

Free Resources for Analytical Chemistry; How Does the Update to Chapter 6 of the EU GMP Guidelines Affect Your Lab?; 7 Free HPLC Tools on the Web; MTS Training Calendar 2013; MTS Helpdesk: Help on... How Many Times Can HPLC System Suitability Tests be Repeated?; New Course: How to Develop Stability Indicating HPLC Methods; MTS Recommends... Using Reference Materials, Quality by Design for Analytical Methods, Forced Degradation Studies in ANDA Submissions; Coming Soon...

 

2012

Summer


Validation and Transfer of Analytical Methods; Implementing Robustness Testing for HPLC Methods;  Tips for Successful Method Transfer; Help on... HPLC Retention Time Change; Help on... Robustness Fcatorial Design for GC; MTS Recommends...; HPLC Training Courses in the UK


2011

December

Free HPLC Calculator - Tool for Method Development; MTS Helpdesk: Help on... Acceptable Variation for HPLC Retention Time; Help on... Assessing Peak Purity Data; USP Chromatographic Columns; 2012 Ireland Training Schedule; New Associate at NSF DBA; MTS Recommends... 'HPLC Columns' by Uwe Neue; MTS Recommends... Measuring pKa by UV/Vis; HPLC Training in Helsinki; HPLC Training in Athlone; Separation Science Europe 2011

October

How to be an Expert on HPLC - Training Courses in Ireland; 5 Step Strategy for HPLC Method Development; Free HPLC Calculator - Update for Column Volume; MTS Helpdesk: Help on... Problem with the first injection from HPLC Vials; Conference Presentation by MTS; How to Troubleshoot HPLC

May

How to Develop HPLC Methods; System Suitability Failures; MTS Helpdesk: Help on... Gradient Programs for HPLC; Help on... Forced Degradation Studies; MTS Recommends... Measuring Volume - Beakers, Cylinders, Erlenmeyer Flasks, & Volumetric Flasks; MTS Recommends...  Chiral Method Development Screening

March

Phenomenex Press Release for HPLC Training Courses in UK; Troubleshooting Tip: Baseline noise; MTS Helpdesk: Help on... 'Dry' solvents for HPLC?; MTS Recommends... LC modelling using DryLab; MTS Recommends...  How to calibrate pipettors; HPLC Training in Belfast

February

MTS Helpdesk: Help on... Equilibration of HPLC Columns Between Gradient Method Injections; HPLC Troubleshooting Training Course in Belfast; MTS Recommends... Using Temperature in LC Method Development; HPLC Training Video Wins Silver Award in Tutorial Competition; MTS Website Updates

 

2010

December

Book sale ends 31st December; MTS Helpdesk: Help on... HPLC Dwell Volume and Dead Volume, Help on... HPLC Baseline Problem; Preparation of Mobile Phase for HPLC; HPLC Training Video Shortlisted in Tutorial Competition; MTS Recommends... How to Weigh Out Small Amounts

November

Huge Savings on HPLC and Method Validation Books: Our End of Year Offer; HPLC Troubleshooting Training Reminder; HPLC e-Learning on CD-ROM for In-house Training; MTS Helpdesk: Help on... Large Peak at the End of a Gradient Analysis; Help on... Developing a HPLC Method for Veterinary Drugs; MTS Recommends... Scaling LC Methods; MTS Recommends... A Review of High Temperature HPLC

October

Free e-Learning Module on HPLC Instruments; HPLC e-Learning Offer Ends 31st October; How to Troubleshoot HPLC; MTS Helpdesk: Help on... Retention Time Variability; MTS Recommends... Quantitative Open Access HPLC; MTS Recommends... 'From Molecule to Medicine' 

September

'How to Troubleshoot HPLC' -New External Training Course; iLearn 'Back-to-School' offer: 20% Discount for bookings made in September & October; Change of Contact Number; MTS Helpdesk: Help on... Retention Time Shifts in Normal Phase HPLC; Help on... Expiry Dates for HPLC Mobile Phase; Help on... Peak Purity Assessment; MTS Recommends... 'Holistic LC strategies, from UHPLC to HPLC and back'; MTS Recommends... Video on Clinical Research

July/August

Tips for Enhancing your Learning Experience; iLearn HPLC e-Learning: Video; MTS Helpdesk: Help on... Investigating OOS &OOT; Lab Tech Guy on a Delicate Problem; MTS Recommends... QbD for Chromatography; MTS Recommends... Headspace GC for Pharmaceutical Analysis

June

iLearn: The e-Learning solution for HPLC Training; MTS Helpdesk: Help on... Number of Injections for HPLC Columns; Help on... Selecting Columns for HPLC; HPLC Calculator; MTS Recommends... 'Kinetic Plots Made Easy'

May

Book Reviews in 'Chemistry World' Magazine; HPLC Calculator: Updated to work out how much mobile phase to prepare for isocratic methods; MTS Helpdesk: Help on... Peak purity by PDA; Help on... Out of Specification (OOS) vs Out of Trend (OOT) Results; Help on... Use of Caffeine for Wavelength Accuracy; MTS Recommends... Reduced Robustness Testing for Analytical methods; Using %RSD Correctly; Ask Lab Tech Guy is now on YouTube!

April

HPLC Calculator: Updated to Include Mobile Phase Buffer Strength; MTS Helpdesk: Help on... Developing a HPLC Method; Help on... TOC vs HPLC for Cleaning Validation Analysis; MTS Recommends... LC Trends at Pittcon; Lab Tech Guy on the Effect of Heating on Volumetric Glassware; And the winner is...

March

 

Free trial of UTrain, online HPLC training for in-house use; HPLC calculator: How can we help you? MTS Helpdesk: Help on... Troubleshooting in pharmaceutical analysis; Updates to the MTS website; MTS Recommends...

 

2009

December

HPLC calculator for pressure conversion; Feedback from free HPLC training video; MTS Helpdesk: Help on... Retention times on different HPLC systems; How was 2009 for you? What do you need to work on in 2010? Lab Tech Guy on resolutions for the New Year

November

HPLC Calculator for column equilibration; Quality by Design for analytical methods; MTS Helpdesk: Help on... HPLC mobile phase composition; Tips for trainers – Icebreakers; Plant a tree with MTS

October

Interpreting a HPLC method; MTS Helpdesk: Help on... Shifting retention times in HPLC analysis; Help on...Measurement of urinary citrate by HPLC; Lab Tech Guy on purge valve frits

September

UTrain: the definitive in-house training solution for basic HPLC; MTS Helpdesk; PocketLab - Free booklet of HPLC data; What is HPLC column efficiency? Lab Tech Guy on 'white powder' on the balance

July/August

Lab Tech Guy on HPLC wash solvents; Learning objectives: Jargon or a trainer's best friend? What to do with outliers in method validation? Can you spot a fake smile? Free training resources in MTS makeover; And the winner is...

June

Free HPLC training video; The training cycle explained; HPLC priming injections; Validation in early phases of drug development; And the winner is; Lab Tech Guy on selecting gloves

May

"I'm a trainer? But that's not in my job description. Is it?"; New book on analytical method validation; Equilibration of HPLC columns; Error and uncertainty in analytical measurement - Part I; Free stuff online; Lab Tech Guy on sharps in the lab

April

Introducing 'Analyse This'; 5 Ways to stretch your 'credit-crunched' training budget; The truth about accuracy in analytical method validation; HPLC column fittings and seating depths; Free list of abbreviations poster; New Book on HPLC for pharmaceutical analysis; Lab Tech Guy on the acetonitrile shortage